
Conditions

Column : Inertsil ODS-3 ( 5 m , 150 4.6mmI.D.)
Flow rate : 1mL/min
Eluent : Methanol/50mM phosphoric acid, 50mM citric acid, 20mg/l EDTA,
400mg/l IPCC-08 (pH3.0 with KOH) = 92/8
IPCC-08 : Sodium 1-Octanesulfonate
Oven Temp. : 30
Detector : ECD 700mV vs. Ag/AgCl
Sample : liquid-liquid extract of urine
Sample Volume : 10 L
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